University of Surrey

Test tubes in the lab Research in the ATI Dance Research

Synthesis and Characterizations of Nickel (II) Oxide Sub-Micro Rods via co-precipitation Methods

Lim, Hui Hui, Amini Horri, Bahman and Salamatinia, Babak (2018) Synthesis and Characterizations of Nickel (II) Oxide Sub-Micro Rods via co-precipitation Methods IOP Conference Series: Materials Science and Engineering, 398 (1), 012033.

[img]
Preview
Text
Synthesis and Characterizations of Nickel (II) Oxide Sub-Micro Rods via co-precipitation Methods.pdf - Version of Record
Available under License Creative Commons Attribution.

Download (901kB) | Preview

Abstract

Co-precipitation method has been used for the synthesis of single crystalline Nickel (II) Oxide sub-micro rods. A two-step method was used to synthesise NiO sub-micro rods, in which the first step was the co-precipitation process Nickel (II) Nitrate with Ammonium Oxalate to form Nickel (II) Oxalate (NiC2O4), which is the precursor for the precipitates. The precipitate precursor then underwent the calcination process to form NiO sub-micro rods. Synthesized materials undergo Field Emission Scanning Electron Microscope (FESEM), particle size measurement via Zetasizer, elemental analysis via Energy-Dispersive X-ray Spectroscopy (EDX), Fourier Transform Infrared Spectroscopy (FT-IR) and Thermogravimetric Analysis (TGA). The morphology of NiO is found to have uniform rod- like crystals with mean z-diameter between 1600 nm to 2600 nm using Zetasizer.

Item Type: Article
Divisions : Faculty of Engineering and Physical Sciences > Chemical and Process Engineering
Authors :
NameEmailORCID
Lim, Hui Hui
Amini Horri, Bahmanb.aminihorri@surrey.ac.uk
Salamatinia, Babak
Date : 2018
DOI : 10.1088/1757-899X/398/1/012033
Copyright Disclaimer : © 2018 The authors. Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI. Published under licence by IOP Publishing Ltd
Depositing User : Clive Harris
Date Deposited : 12 Oct 2018 12:30
Last Modified : 12 Dec 2018 16:53
URI: http://epubs.surrey.ac.uk/id/eprint/849654

Actions (login required)

View Item View Item

Downloads

Downloads per month over past year


Information about this web site

© The University of Surrey, Guildford, Surrey, GU2 7XH, United Kingdom.
+44 (0)1483 300800