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Synthesis and characterization of Co@Ag core-shell nanoparticles

Garcia-Torres, J, Vallés, E and Gómez, E (2010) Synthesis and characterization of Co@Ag core-shell nanoparticles Journal of Nanoparticle Research, 12 (6). pp. 2189-2199.

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Abstract

A micellar method has been used to prepare silver-coated cobalt (Co@Ag) nanoparticles. The synthesized particles have been deeply characterized by several methods, i.e., XRD, UV-Vis, TEM, XPS, and electrochemical techniques. There is every indication that the obtained particles show a truly core-shell structure. All the nanoparticles obtained under different conditions are in the size range 3-5 nm. High-resolution TEM (HRTEM), Fast Fourier Transformation (FFT), and Selected Area Electron Diffraction (SAED) indicated that the presence of hcp-Co and fcc-Ag, in which cobalt is located in the central area; meanwhile silver is at the edges of the nanoparticle. The absorption band of the Co@Ag colloid shifts to a longer wavelength and broadens relative to that of pure silver colloid. Voltammetric characterization allowed to determine the coverage of the cobalt core. © 2009 Springer Science+Business Media B.V.

Item Type: Article
Authors :
NameEmailORCID
Garcia-Torres, JUNSPECIFIEDUNSPECIFIED
Vallés, EUNSPECIFIEDUNSPECIFIED
Gómez, EUNSPECIFIEDUNSPECIFIED
Date : 1 August 2010
Identification Number : 10.1007/s11051-009-9784-x
Depositing User : Symplectic Elements
Date Deposited : 17 May 2017 13:20
Last Modified : 17 May 2017 13:20
URI: http://epubs.surrey.ac.uk/id/eprint/838856

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