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Silenes as novel synthetic reagents: identification of a practical method for silene generation and trapping.

Berry, MB, Griffiths, RJ, Sanganee, MJ, Steel, PG and Whelligan, DK (2004) Silenes as novel synthetic reagents: identification of a practical method for silene generation and trapping. Org Biomol Chem, 2 (16). pp. 2381-2392.

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Abstract

The elucidation of a robust and reliable sequence for the generation of highly reactive transient silenes from simple aldehydes is described. The key step involves a silyl-modified Peterson olefination which critically depends on the presence of a sub-stoichiometric amount of soluble lithium salts (LiBr).

Item Type: Article
Authors :
NameEmailORCID
Berry, MBUNSPECIFIEDUNSPECIFIED
Griffiths, RJUNSPECIFIEDUNSPECIFIED
Sanganee, MJUNSPECIFIEDUNSPECIFIED
Steel, PGUNSPECIFIEDUNSPECIFIED
Whelligan, DKd.whelligan@surrey.ac.ukUNSPECIFIED
Date : 21 August 2004
Identification Number : https://doi.org/10.1039/B404166F
Uncontrolled Keywords : Indicators and Reagents, Lithium, Magnetic Resonance Spectroscopy, Models, Chemical, Molecular Structure, Silene, Solubility, Temperature
Depositing User : Symplectic Elements
Date Deposited : 17 May 2017 12:07
Last Modified : 17 May 2017 15:01
URI: http://epubs.surrey.ac.uk/id/eprint/834107

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